16) Organic synthesis

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How to separate the organic layer?

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Place a second concial flask under the separating funnel to collect the other layer.

Add some water to see which layers increase in volume, this is the aqueous layer.

Allow the layers to settle.

Ensure that the tap of the separating tunnel is closed.

You will now have one concial flask containing the organic layer and another with the aqueous layer in.

Pour the mixture of liquids into the separating funnel, place a stopper at the top and invert to mix the contents.

Place a concial flask under the separating funnel, remove the stopper and open the tap until the whole layer has left the funnel.

Once the organic product has been identified, the two layers are separated using a separation funnel.


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